The article discusses a novel approach to the electrochemical exfoliation of graphite to produce two-dimensional graphene-like materials. The use of aqueous ammonium hydrogen carbonate solution as an electrolyte results in the creation of a porous two-dimensional structure. This exfoliated product exhibits long-term stability, being dispersible in water for over five years. The porous surface of the material provides an excellent platform for supporting molecular metal complexes, making it an effective heterogeneous electrocatalyst for hydrogen production. This innovative method opens up possibilities for creating unique exfoliated products with enhanced functionality, particularly in the field of carbon materials and nanocomposites. The study highlights the potential of this approach in advancing the development of materials for various applications requiring stable and efficient electrocatalysts.