The study focused on hydrogen production through water splitting using nano-ferrites as a photocatalyst, ethanol as a sacrificial donor, and Pt as a co-catalyst. Nano-ferrites exhibited a significantly higher hydrogen evolution rate and yield under visible light compared to commercial iron oxide. The research explored the influence of different photoreactor configurations on hydrogen evolution, showing a substantial increase in rate by adjusting the setup. Furthermore, nano-ferrites demonstrated stability in hydrogen production over 30 hours, indicating their potential for practical applications. Factors affecting hydrogen yield, such as photocatalyst dose and illumination conditions, were investigated to optimize the process. The results highlight the promising performance of nano-ferrites in photocatalytic hydrogen production and emphasize the importance of reaction conditions and catalyst design in enhancing efficiency and stability.